Panacetin Lab Write Up

research testing groundoratory report card Format for Separating the Components of Panacetin (2) and Recrystallization and Melting Point Measurement Identifying the Components of Panacetin (3). laboratory Notebook Title and Date Objective apologise the purpose of the try out and how you plan to accomplish it. proficiency showing the use of separatory funnel and evaporation of root setup Reaction(s) Include the main reaction for the experiment and isolation scheme somatogenetic Data tendency the molecular weight, melt point, boiling point, density, solubility, and hazards of all clever chemicals used in the experiment.Data/Observations Your observations of the experiment, a. cargo of sign panacetin sample. b. tip of sucrose collected. c. Weight of aspirin collected. d. Weight of terra incognita sharpen isolated e. Weight of recrystallized unappreciated compound f. Melting point range of recrystallized nameless compound. g. tender loving care sketches with appropriat e entropy for Rf calculations (Clearly set each column of spots on the varlet so I know what it is) h. involved melting point based on development from TLC Final Report ? Title Page.Include (1) the epithet of the experiment, (2) your name, (3) the due date, and (4) the date submitted ? Purpose of the Experiment. ? Background/ apparatus ( 1 page) ? Discuss extraction theory and explain the general operation of the equipment ? formulate the theory hind end isolation scheme ? justify the purpose of recrystillization ? map reference the subroutine (i. e. text or handout) and either changes that deviated from the original reference ? Data and Results o Physical description for substance(s) isolated o Weight of initial panacetin sample. o o o o o o o o oWeight of sucrose collected. Weight of aspirin collected. Weight of unknown compound isolated Weight of recrystallized unknown compound Melting point range of recrystallized unknown compound. Mixed melting point based on informa tion from TLC TLC Cross reference with lab notebook Rf values from TLC (including the firmness used) Percent recovery of sucrose, aspirin and your unknown ? Calculations Show sample calculations of the percent recoveries of sucrose, aspirin and your unknown and Rf calculations. ? Discussion. What was the identity of your unknown?Explain in stage how you determined it, comparing the data you obtained with known values. Explain any discrepancies. (1 page) ? Conclusion brief statement with concluding conclusion (restating the goal of the lab and summarizing important data showing that the goal was or was not achieved) ? Excercises Lab 2 questions 1,3,5 Lab 31 and 2 Additional Question Where in the separation procedure could you lose one or more of the Panacetin components? Explain which component could be lost in which step. thin trace amounts left in containers, or vociferous spills.